Pyridine → 2-Nitrobenzamide

Participants

Reaction Conditions

Reaction Steps

The free amine obtained from the BOC deprotection step was dissolved in pyridine and nitrobenzoyl chloride (1.2 equiv.) was added to this solution. After stirring for 2 h at 90° C., the reaction mixture was concentrated and the resulting crude product was used for the next step without further purification.

Provenance & Evidence