HCID 117760182, compound → HCID 117759897, compound

Participants

Reaction Steps

To a solution of 2,4-bis(benzyloxy)-2′-fluoro-5′-methoxy-1,1′-biphenyl (23.9 g) in THF (300 mL) was added 10% palladium-activated carbon (9.60 g) and, under a hydrogen atmosphere, the mixture was stirred at room temperature for 2 hr. The reaction mixture was filtered through celite, and the filtrate was concentrated under reduced pressure to give the title compound (21.8 g) as a colorless crude oil. This compound was used for the next step without further purification.

Provenance & Evidence