HCID 117760058, compound → HCID 117760038, compound

Participants

Reaction Steps

To a solution of 2-(3,6-dihydro-2H-pyran-4-yl)-2′-fluoro-5′-methoxybiphenyl-4-ol (138 mg) in methanol (3.0 mL) was added 10% palladium-carbon (55 mg), and the mixture was stirred under a hydrogen atmosphere at room temperature for 1 hr. The mixture was filtered through celite, and the filtrate was concentrated under reduced pressure. The residue was directly used for the next step.

Provenance & Evidence