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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1049722Generated: November 2, 2026

2,3-Dimethylbenzoic acid → HCID 117699240, compound

https://huagongshe.com/reaction/1049722

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,3-Dimethylbenzoic acidHCID 11782—
Reactant2,3-Dimethylbenzoyl chlorideHCID 2800899—
ReactantHCID 117699136HCID 117699136—
ProductHCID 117699240HCID 11769924092%

Reaction Steps

2,3-Dimethylbenzoic acid (21 mg, 0.140 mmol) was made into acid chloride in a conventional manner. By using 1-(4-aminophenyl)-6-methyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione (20 mg, 0.071 mmol) mentioned above, and 2,3-dimethylbenzoyl chloride mentioned above, the title compound (27 mg, yield 92%) was obtained in the same manner as that of Example 1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09382236B2
Source datasetuspto-grants-2016_07
ORD IDord-76eec9d5d57b437a819c53bffe340acb
Source noteuspto-grants-2016_07