HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethylbenzoic acid → HCID 117699240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethylbenzoic acid | HCID 11782 | — |
| Reactant | 2,3-Dimethylbenzoyl chloride | HCID 2800899 | — |
| Reactant | HCID 117699136 | HCID 117699136 | — |
| Product | HCID 117699240 | HCID 117699240 | 92% |
Reaction Steps
2,3-Dimethylbenzoic acid (21 mg, 0.140 mmol) was made into acid chloride in a conventional manner. By using 1-(4-aminophenyl)-6-methyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione (20 mg, 0.071 mmol) mentioned above, and 2,3-dimethylbenzoyl chloride mentioned above, the title compound (27 mg, yield 92%) was obtained in the same manner as that of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-76eec9d5d57b437a819c53bffe340acb |
| Source note | uspto-grants-2016_07 |