HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodobenzoic acid → HCID 117720140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodobenzoic acid | HCID 6941 | — |
| Reactant | 2-Iodobenzoyl chloride | HCID 69112 | — |
| Reactant | HCID 117699240 | HCID 117699240 | — |
| Product | HCID 117720140 | HCID 117720140 | 87% |
Reaction Steps
2-Iodobenzoic acid (34 mg, 0.137 mmol) was made into acid chloride in a conventional manner. By using 1-(4-aminophenyl)-6,7-dimethyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione (20 mg, 0.068 mmol) obtained in Example 56, and 2-iodobenzoyl chloride mentioned above, the title compound (31 mg, yield 87%) was obtained in the same manner as that of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-a3119bd403454e06b27dd1df811dc6a1 |
| Source note | uspto-grants-2016_07 |