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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1049737Generated: November 2, 2026

2-Iodobenzoic acid → HCID 117720140, compound

https://huagongshe.com/reaction/1049737

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Iodobenzoic acidHCID 6941—
Reactant2-Iodobenzoyl chlorideHCID 69112—
ReactantHCID 117699240HCID 117699240—
ProductHCID 117720140HCID 11772014087%

Reaction Steps

2-Iodobenzoic acid (34 mg, 0.137 mmol) was made into acid chloride in a conventional manner. By using 1-(4-aminophenyl)-6,7-dimethyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione (20 mg, 0.068 mmol) obtained in Example 56, and 2-iodobenzoyl chloride mentioned above, the title compound (31 mg, yield 87%) was obtained in the same manner as that of Example 1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09382236B2
Source datasetuspto-grants-2016_07
ORD IDord-a3119bd403454e06b27dd1df811dc6a1
Source noteuspto-grants-2016_07