HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Chlorophenyl)methanesulfonyl chloride → HCID 117699045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Chlorophenyl)methanesulfonyl chloride | HCID 2757801 | — |
| Reactant | HCID 117699460 | HCID 117699460 | — |
| Product | HCID 117699045 | HCID 117699045 | 21.5% |
Reaction Steps
By using 1-(4-aminophenyl)-7-methoxy-1H-1,5-benzodiazepine-2,4(3H,5H)-dione (65 mg, 0.22 mmol), and 2-chlorobenzylsulfonyl chloride (74 μL, 0.33 mmol), the title compound (23 mg, yield 13%) was obtained in the same manner as that of Example 145.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-8f68296e0f4a4972aa46a0af3c1afd0c |
| Source note | uspto-grants-2016_07 |