4-Heptanone → HCID 178444008, compound

HRID 1049849Notes

Reaction equation

HRID 1049849 reaction equation
[NH:1]([C:3]1[N:8]=[CH:7][N:6]=[C:5]([OH:9])[CH:4]=1)[NH2:2].[CH3:10][CH2:11][CH2:12][C:13](=O)[CH2:14][CH2:15][CH3:16]>>[CH3:10][CH2:11][CH2:12][C:13](=[N:2][NH:1][C:3]1[N:8]=[CH:7][N:6]=[C:5]([OH:9])[CH:4]=1)[CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 312464-HeptanoneHCID 178514311HCID 178514311, compound

Product 1

HCID 178444008HCID 178444008, compound

Procedure

10.0 g (79.3 mmol) 6-hydrazinopyrimidin-4-ol (CAS-No: 29939-37-5) were transformed in analogy to intermediate example 1c using heptan-4-one to give after working up and purification 13.5 g (77%) of the title compound.

Workup

  1. customto give
  2. custompurification 13.5 g (77%) of the title compound

Sources & evidence

ORD record
ord-e2d9441c937d43028e9dc9ebf1b73381
Source dataset
uspto-grants-2016_07
Patent number
US09382255B2

Reaction notes

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