Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 117703949 | HCID 117703949 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 117704022 | HCID 117704022 | — |
Reaction Steps
2-Acetylamino-5-benzenesulfonyl-4-methyl-thiophene-3-carboxylic acid amide (980 mg 2.9 mmol) is dissolved in a mixture of 6 M aqueous HCl and 1,4-dioxane (1:1, 10 mL). This mixture is then heated at 80° C. for 6 h, and concentrated by evaporation to yield a residue that is as such.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09382254B2 |
|---|
| Source dataset | uspto-grants-2016_07 |
|---|
| ORD ID | ord-71273d99ffd944e596f5d1e9ffbadd6b |
|---|
| Source note | uspto-grants-2016_07 |
|---|
