HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1,1'-(methylsilylene)bis- → ({bicyclo[2.2.1]hept-5-en-2-yl}methoxy)(methyl)diphenylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1,1'-(methylsilylene)bis- | HCID 69893 | — |
| Reactant | 6814-81-9 | HCID 20273145 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Product | ({bicyclo[2.2.1]hept-5-en-2-yl}methoxy)(methyl)diphenylsilane | HCID 23448607 | — |
Reaction Steps
and reacting norbornene methanol (IB) with methyldiphenylsilane in the presence of a suitable solvent and potassium tert-butoxide to obtain (bicyclo[2.2.1]hept-5-en-2-ylmethoxy)(methyl)diphenylsilane (VB) of at least 99.5 percent purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382271B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-54a9faded0e9486c8595292d63b7d3e4 |
| Source note | uspto-grants-2016_07 |