HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 71268826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 71268944 | HCID 71268944 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 71268826 | HCID 71268826 | — |
Reaction Steps
Tert-butyl 4-(4-(2-(4-(methoxycarbonyl)phenyl)-5-oxo-5,6-dihydropyrimido[4,5-d]pyridazin-4-ylamino)benzyl)piperazine-1-carboxylate (0.1 g, 0.175 mmol) was dissolved in dioxane.HCl (5 mL) and stirred at room temperature for 1.5 hours. The solid obtained was filtered and the residue washed with EtOAc and dried to give the desired product (40 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382277B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-8aaf59ddb1b9416398f1e09f9a56650b |
| Source note | uspto-grants-2016_07 |