HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide potassium salt → HCID 90295825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Reactant | HCID 131736050 | HCID 131736050 | — |
| Product | HCID 90295825 | HCID 90295825 | 79.4% |
Reaction Steps
Using compound ((3R,3aS)-1-oxo-7-(2-oxopiperidin-1-yl)-1,3,3a,4-tetrahydrobenzo[b]oxazolo[3,4-d][1,4]oxazin-3-yl)methylmethanesulfonate (0.774 g, 1.95 mmol), phthalimide potassium (0.542 g, 2.93 mmol) as starting materials, preparation following the method as described in Example 1(d) afforded white solid 0.693 g, yield: 79.3%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382265B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-88adb7126d70487d85699ee1ac08ee64 |
| Source note | uspto-grants-2016_07 |