HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide potassium salt → HCID 90295627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Reactant | HCID 90295545 | HCID 90295545 | — |
| Product | HCID 90295627 | HCID 90295627 | 79.1% |
Reaction Steps
Using compound 4-((3R,3 aS)-3-((methylsulfonyloxy)methyl)-1-oxo-1,3,3a,4-tetrahydrobenzo[b]oxazolo[3,4-d][1,4]oxazin-7-yl)-3-oxopiperazin-1-carboxylic acid benzyl ester (0.916 g, 1.725 mmol), and phthalimide potassium (0.479 g, 2.558 mmol) as starting materials, preparation following the method as described in Example 1 (d) afforded white solid 0.794 g, yield: 79.1%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382265B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-bd86571d862344d0bdd0f0e26dce66e8 |
| Source note | uspto-grants-2016_07 |