HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide potassium salt → HCID 90295592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Reactant | HCID 90295553 | HCID 90295553 | — |
| Reactant | HCID 131736055 | HCID 131736055 | — |
| Product | HCID 90295592 | HCID 90295592 | 82.1% |
Reaction Steps
Using compound ((3R,3 aR)-1-oxo-7-(3-oxomorpholin-4-yl)-1,3,3a,4-tetrahydrobenzo[b]oxazolo[3,4-d][1,4]oxazin-3-yl)methylmethanesulfonate (2.98 g, 7.48 mmol) prepared above in (a) and phthalimide potassium (2.08 g, 11.22 mmol) as starting materials, preparation following the method as described in Example 1 (d) afforded white solid 2.76 g, yield: 82.1%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382265B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-2845f116079e4fe2a3b0ebcdfd0f2415 |
| Source note | uspto-grants-2016_07 |