HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 4-Bromo-2,6-dinitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 2,6-Dinitroaniline | HCID 69070 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-Bromo-2,6-dinitroaniline | HCID 3746608 | 86% |
Reaction Steps
A mixture comprising 247.5 g (1.35 mol) 2,6-dinitroaniline, 2.5 L acetic acid and 250 mL bromine was heated to 100° C. for a few minutes. After cooling, the formed crystals were filtered and washed with n-hexane to give 304 g (86%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388140B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-71fb586d4a5d439f89dfb3327ed607a9 |
| Source note | uspto-grants-2016_07 |