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Aniline → 1-(t-butylamino)-N-(2-methyl-5-(phenylcarbamoyl)phenyl)isoquinoline-5-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | 1-(t-butylamino)-N-(2-methyl-5-((3-(trifluoromethyl)phenyl)carbamoyl)phenyl)isoquinoline-5-carboxamide | HCID 118090796 | — |
| 生成物 | 1-(t-butylamino)-N-(2-methyl-5-(phenylcarbamoyl)phenyl)isoquinoline-5-carboxamide | HCID 118090883 | 3% |
反応手順
The procedures of Steps (1), (2) and (3) of Example 2 were repeated step by step, except for using aniline instead of 3-trifluoro-aniline in Step (1) of Example 2 to obtain the title compound (1.2 mg, 3%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09388165B2 |
| 出典データセット | uspto-grants-2016_07 |
| ORD ID | ord-d225905776ff4b6e8f67410e46e36948 |
| 出典メモ | uspto-grants-2016_07 |