HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyrimidine → HCID 86631773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyrimidine | HCID 7978 | — |
| Reactant | HCID 53434504 | HCID 53434504 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86631773 | HCID 86631773 | — |
Reaction Steps
4.6 g 4-[bromo(phenyl)acetyl]benzaldehyde and 1.64 g pyrimidin-2-amine are stirred in 140 ml DMF at 90° C. for 4 h. The DMF is evaporated and the residue suspended in ethylacetate over night, collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09387204B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-6b7784d17daf4937ad2e9fdca44ad483 |
| Source note | uspto-grants-2016_07 |