HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 4-(2-(3,5-Dimethoxyphenethyl)-5H-pyrrolo[2,3-b]pyrazin-6-yl)-N,N-dimethylpicolinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 4-(2-(3,5-Dimethoxyphenethyl)-5H-pyrrolo[2,3-b]pyrazin-6-yl)picolinic acid | HCID 89963589 | — |
| Product | 4-(2-(3,5-Dimethoxyphenethyl)-5H-pyrrolo[2,3-b]pyrazin-6-yl)-N,N-dimethylpicolinamide | HCID 73058328 | — |
Reaction Steps
The compound was prepared by using procedures analogous to those described for the synthesis of Example 73, Step 3 starting from 4-{2-[2-(3,5-dimethoxyphenyl)ethyl]-5H-pyrrolo[2,3-b]pyrazin-6-yl}pyridine-2-carboxylic acid and N,N-dimethyl amine (2.0 M in THF). LCMS calculated for C24H26N5O3 (M+H)+: m/z=432.2. Found 432.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388185B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-7aa16fb2c7e54155bb289bb8b8ee1fbd |
| Source note | uspto-grants-2016_07 |