HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5-bromopyridine → HCID 57843410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5-bromopyridine | HCID 817681 | — |
| Reactant | 2,4-Difluorobenzenesulfonyl Chloride | HCID 2734273 | — |
| Product | HCID 57843410 | HCID 57843410 | 102.1% |
Reaction Steps
5-Bromopyridin-3-amine (500 mg, 2.89 mmol) was treated with 2,4-difluorobenzene-1-sulfonyl chloride (390 μl, 2.90 mmol) according to the method described in Preparation 15b to give 1.03 g (100% yield) of the title compound as an oil. Purity 74%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388189B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-74e52565e44544c8913f8d17fd336f2d |
| Source note | uspto-grants-2016_07 |