HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → N-(3-Iodo-5-morpholinophenyl)methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 3-Iodo-5-morpholinoaniline | HCID 90102755 | — |
| Product | N-(3-Iodo-5-morpholinophenyl)methanesulfonamide | HCID 90102530 | 105% |
Reaction Steps
3-Iodo-5-morpholinoaniline (279 mg, 0.76 mmol) was treated with methanesulfonyl chloride (82 μl, 1.06 mmol) according to the method described in Preparation 15b to give 305 mg (95% yield) of the title compound as an oil. Purity 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388189B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-609383405f7f4e80ba1c642cfa5e7e9c |
| Source note | uspto-grants-2016_07 |