HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 90103295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 4-Bromo-1H-indazol-6-amine | HCID 24728067 | — |
| Product | HCID 90103295 | HCID 90103295 | 61.5% |
Reaction Steps
4-Bromo-1H-indazol-6-amine (500 mg, 2.36 mmol) was treated with methanesulfonyl chloride (130 μl, 1.68 mmol) and triethylamine (49 μl, 3.55 mmol) according to the method described in Preparation 15b. The residue was purified using SP1® Purification System to give 300 mg (49% yield) of the title compound. Purity 80%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388189B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-3020f2c059ce401a874eb1547830ad4e |
| Source note | uspto-grants-2016_07 |