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HRID1052642

反应详情

EQUATION

反应方程式

HRID 1052642 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)Cc1ccc(F)cc1
HCID2759108

(4-fluorophenyl)methanesulfonyl Chloride

C7H6ClFO2S

结构：COc1cc(N)cc(B2OC(C)(C)C(C)(C)O2)c1
HCID90102627

3-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

C13H20BNO3

PRODUCTS

生成物

1
结构：COc1cc(NS(=O)(=O)Cc2ccc(F)cc2)cc(B2OC(C)(C)C(C)(C)O2)c1
HCID90102918

未命名化合物

收率 94%

PROCEDURE

实验过程

3-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline (822 mg, 3.29 mmol), was treated with (4-fluorophenyl)methanesulfonyl chloride (1.03 ml, 4.93 mmol) according to the method described in Preparation 15b to give 1.26 g (94% yield) of the title compound. Purity 97%.