HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-fluorophenyl)methanesulfonyl Chloride → HCID 90102918, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-fluorophenyl)methanesulfonyl Chloride | HCID 2759108 | — |
| Reactant | 3-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine | HCID 90102627 | — |
| Product | HCID 90102918 | HCID 90102918 | 94% |
Reaction Steps
3-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline (822 mg, 3.29 mmol), was treated with (4-fluorophenyl)methanesulfonyl chloride (1.03 ml, 4.93 mmol) according to the method described in Preparation 15b to give 1.26 g (94% yield) of the title compound. Purity 97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388189B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-f986833e3ed242739dd69239baf0ce5f |
| Source note | uspto-grants-2016_07 |