反应详情

Was prepared in the same manner as described in General Procedure Example 2, using (Z)-methyl N-3-methylbut-2-enoylpyrrolidine-1-carbimidothioate (3.69 g, 16.3 mmol, Eq: 1.00) and hydrazine 1M in THF (16.3 ml, 16.3 mmol, Eq: 1.00). Chromatography afforded 5-(2-Methyl-propenyl)-3-pyrrolidin-1-yl-1H-[1,2,4]triazole (695 mg, 22.2%) as white waxy solid. MS: m/z=193.1 (M+H+)

1. customWas prepared in the same manner