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HRID1054965

反应详情

EQUATION

反应方程式

HRID 1054965 的结构方程式

REACTANTS

反应物

2
结构：Cn1nc(N2CCCC2)nc1C=O
HCID83875440

未命名化合物

结构：Clc1ccc2nc(C[P+](c3ccccc3)(c3ccccc3)c3ccccc3)nn2c1.[Cl-]
HCID90025615

未命名化合物

PRODUCTS

生成物

1
结构：Cn1nc(N2CCCC2)nc1C=Cc1nc2ccc(Cl)cn2n1
HCID123548203

未命名化合物

收率 91.1%

PROCEDURE

实验过程

The desired product was prepared in analogy to Example 1 g) from ((6-chloro-[1,2,4]triazolo[1,5-a]pyridin-2-yl)methyl)triphenylphosphonium chloride (170 mg, 366 μmol, Eq: 1.00) and 1-methyl-3-(pyrrolidin-1-yl)-1H-1,2,4-triazole-5-carbaldehyde (66.0 mg, 366 μmol, Eq: 1.00). 110 mg (91%) of the desired product were obtained as a light yellow solid. MS: m/z=330.4 (M+H+)