HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90032734, compound → HCID 72704900, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90032734 | HCID 90032734 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 72704900 | HCID 72704900 | 62.5% |
Reaction Steps
(E)-5,7,8-Trimethyl-2-(2-(1-methyl-3-(pyrrolidin-1-yl)-1H-1,2,4-triazol-5-yl)vinyl)-[1,2,4]triazolo[1,5-c]pyrimidine (32 mg) and Pd/C (10 mg) were stirred in ethanol (0.4 ml) under hydrogen for 1 h. The mixture was filtered and concentrated to give the product (20 mg, 62.5%) as a white waxy solid. MS: m/z=341.4 (M+H+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394311B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-b09f844228384a14bc5aa85bf13b36a7 |
| Source note | uspto-grants-2016_07 |