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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1054974Generated: November 1, 2026

HCID 90032734, compound → HCID 72704900, compound

https://huagongshe.com/reaction/1054974

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 90032734HCID 90032734—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 72704900HCID 7270490062.5%

Reaction Steps

(E)-5,7,8-Trimethyl-2-(2-(1-methyl-3-(pyrrolidin-1-yl)-1H-1,2,4-triazol-5-yl)vinyl)-[1,2,4]triazolo[1,5-c]pyrimidine (32 mg) and Pd/C (10 mg) were stirred in ethanol (0.4 ml) under hydrogen for 1 h. The mixture was filtered and concentrated to give the product (20 mg, 62.5%) as a white waxy solid. MS: m/z=341.4 (M+H+)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09394311B2
Source datasetuspto-grants-2016_07
ORD IDord-b09f844228384a14bc5aa85bf13b36a7
Source noteuspto-grants-2016_07