HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 72705474, compound → HCID 178427934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 72705474 | HCID 72705474 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 178427934 | HCID 178427934 | 100% |
Reaction Steps
6,8-Dichloro-2-(2-(1-(4-methoxybenzyl)-5-(pyrrolidin-1-yl)-1H-1,2,4-triazol-3-yl)ethyl)-5-methyl-[1,2,4]triazolo[1,5-a]pyridine (17 mg, 35.0 μmol, Eq: 1.00) in trifluoroacetic acid (539 μl) was heated 3 h under reflux. The product (12.8 mg, 100%) was obtained as a white solid by preparative HPLC. MS: m/z=366.2 (M+H+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394311B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-f7c5a5f830d444e5b5ed5d99e9f36f4e |
| Source note | uspto-grants-2016_07 |