HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90017318, compound → HCID 90018297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90017318 | HCID 90017318 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 90018297 | HCID 90018297 | — |
Reaction Steps
N-(4-Methoxybenzyl)-6-methyl-3-(trifluoromethyl)pyridin-2-amine (100 mg, 338 μmol, Eq: 1.00) in trifluoroacetic acid (2 ml) was heated under reflux for 30 min. The mixture was concentrated. The crude product (120 mg, pink solid) was used in the next step without further purification. MS: m/z=218.2 (M+H+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394311B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-f692e6c33e7346948fe289090a178efd |
| Source note | uspto-grants-2016_07 |