HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 13719288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methyl 4-methyl-3-oxopentanoate | HCID 2759969 | — |
| Product | HCID 13719288 | HCID 13719288 | — |
Reaction Steps
0.69 mol (100 g) of 4-methyl-3-oxovaleric acid methyl ester and 309 ml 33% dimethylamine in ethanol (about 1.73 mol dimethylamine) were stirred in a pressure reactor for 2 hours at 110° C. After cooling, the solvents were distilled on a rotary evaporator. After drying, 93 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394324B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-ed7d0995b96c418d9762d4ff3c0ee294 |
| Source note | uspto-grants-2016_07 |