Saccharin → Acetate Saccharin

HRID 1055257Notes

Reaction equation

HRID 1055257 reaction equation
[C:1]([O-:4])(=[O:3])[CH3:2].[Na+].[S:6]1([C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:10](=[O:11])[NH:9]1)(=[O:8])=[O:7].[Na].S1(C2C(=CC=CC=2)C(=O)N1)(=O)=O.[OH-].[Na+]>O>[C:1]([O-:4])(=[O:3])[CH3:2].[S:6]1([C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:10](=[O:11])[NH:9]1)(=[O:7])=[O:8]

Participants

6

Reactant 4

HCID 5143SaccharinHCID 14798Sodium HydroxideHCID 517045Sodium AcetateHCID 24181110Benzosulfinide sodium; Garantose sodium

Product 1

HCID 86648896Acetate Saccharin

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Into a sterile 15 mL plastic centrifuge tube was placed 0.0021 g decapeptide, 0.0016 g sodium acetate, 0.0094 g sodium saccharin and 7.0 g sterile water. The pH was adjusted using only the necessary amount of acid saccharin to a pH of 4. Into a new 15 mL plastic centrifuge tube was placed 3.5 mL of a pH 4 solution. The pH was adjusted using only the necessary amount of 1.0N NaOH to a final pH of 7.

Workup

  1. customInto a sterile 15 mL plastic centrifuge tube was placed
  2. customInto a new 15 mL plastic centrifuge tube was placed

Sources & evidence

ORD record
ord-87f72591ead84b318e463751061415ac
Source dataset
uspto-grants-2016_07
Patent number
US09394339B2

Reaction notes

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