Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1055266Generated: November 1, 2026

Trifluoroacetic acid → HCID 86711157, compound

https://huagongshe.com/reaction/1055266

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86711158HCID 86711158—
SolventDichloromethaneHCID 6344—
ProductHCID 86711157HCID 86711157—

Reaction Steps

A solution of N-(3-((3-(2-(4-(6-fluorobenzo[d]isoxazol-3-yl)piperidin-1-yl)ethyl)-2-methyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidin-9-yl)oxy)propyl)pivalamide, prepared as described in Step A, (1.482 g, 2.54 mmol) in dichloromethane (10 mL) and trifluoroacetic acid (5 mL) was stirred for 1 h at room temperature. The reaction mixture was purified on a Porapak CX column to give the title compound which was used without further purification in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09394354B2
Source datasetuspto-grants-2016_07
ORD IDord-987a0d2c9d5748b3b24f173af09ae126
Source noteuspto-grants-2016_07