HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10516606, compound → HCID 89699857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10516606 | HCID 10516606 | — |
| Reactant | 1-Bromo-2,3-dimethyl-5-nitrobenzene | HCID 20680442 | — |
| Product | HCID 89699857 | HCID 89699857 | — |
Reaction Steps
Analogously to Example 13A/Step 1, two batches of 100 mg (0.36 mmol) and of 1.50 g (5.43 mmol), respectively, of the compound of Example 4A and 92 mg (0.40 mmol) and 1.37 g (5.97 mmol), respectively, of 1-bromo-2,3-dimethyl-5-nitrobenzene gave a total of 1.31 g (23% of theory) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394309B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-73bf6f977b2e47358c847cdc1d702859 |
| Source note | uspto-grants-2016_07 |