HRID1055706

反应详情

EQUATION

反应方程式

HRID 1055706 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

At 80° C., 25 mg (0.025 mmol, 57% pure) of the compound from Example 50A were stirred in 0.5 ml of trifluoroacetic acid for 6 h. After concentration of the mixture under reduced pressure, the residue was purified by preparative HPLC (Method 11). This gave 6.0 mg (53% of theory) of the title compound.

WORKUP

后处理

  1. customAfter concentration of the mixture under reduced pressure, the residue was purified by preparative HPLC (Method 11)