HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Tert-butylpyridine-4-carboxylic acid → HCID 89699997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Tert-butylpyridine-4-carboxylic acid | HCID 693292 | — |
| Reactant | 4-Methyl-3-[6-(pyridin-3-yl)-1H-imidazo[1,2-b]pyrazol-1-yl]aniline | HCID 89700023 | — |
| Product | HCID 89699997 | HCID 89699997 | — |
Reaction Steps
60 mg (0.21 mmol) of the compound of Example 6A and 37 mg (0.21 mmol) of 2-tert-butyliso-nicotinic acid were reacted and worked up analogously to the procedure of Example 33, except that in this case the reaction time was 16 h. This gave 13 mg (96% pure, 13% of theory) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394309B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-762017741e944bcd95554c67d8a59aea |
| Source note | uspto-grants-2016_07 |