HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89699811, compound → HCID 89699706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89699811 | HCID 89699811 | — |
| Reactant | 4-Methyl-3-[6-(pyridin-3-yl)-1H-imidazo[1,2-b]pyrazol-1-yl]aniline | HCID 89700023 | — |
| Product | HCID 89699706 | HCID 89699706 | — |
Reaction Steps
Analogously to the process described in Example 26, 80 mg (0.276 mmol) of the compound of Example 6A and 60 mg (0.276 mmol) of the compound of Example 73A gave 115 mg (82% of theory, 96% pure) of the title compound. In this case, the reaction time was 1 h. Final trituration of the product was carried out using a mixture of 10 ml of pentane and 2 ml of diisopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394309B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-ae6ef995d1fd4a0f9310dea8e02e2c68 |
| Source note | uspto-grants-2016_07 |