HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyano-5-(pentafluoro-lambda6-sulphanyl)benzoic acid → HCID 89700174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyano-5-(pentafluoro-lambda6-sulphanyl)benzoic acid | HCID 89699812 | — |
| Reactant | HCID 89699966 | HCID 89699966 | — |
| Product | HCID 89700174 | HCID 89700174 | — |
Reaction Steps
Analogously to the process described in Example 155, 37 mg (0.109 mmol) of the compound of Example 82A and 28 mg (0.104 mmol) of the compound of Example 23A were reacted to give 9 mg (15% of theory) of the title compound. Here, preparative HPLC purification was carried out according to Method 37.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394309B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-6c32df39ac6c4632bf9fd485dc6338ba |
| Source note | uspto-grants-2016_07 |