3-[7-Fluoro-6-(pyridin-3-yl)-1H-imidazo[1,2-b]pyrazol-1-yl]-4-methylaniline → HCID 89699742, compound

Participants

Reaction Steps

Analogously to the process described in Example 126, 60 mg (0.195 mmol) of the compound of Example 83A and 53 mg (0.195 mmol) of the compound of Example 23A gave 61 mg (55% of theory) of the title compound. The product obtained from the preparative HPLC purification was dissolved in a little methanol and passed through a bicarbonate cartridge (from Polymerlabs, Stratospheres SPE, PL-HCO3 MP SPE, capacity 0.9 mmol). After concentration of the eluate, the residue was dried under high vacuum.

Provenance & Evidence