Pyridine → 1-Chloroethyl Cyclohexyl Carbonate

Participants

Reaction Steps

The title compound was prepared according to the procedure as described in Example 26 step 1 using a solution of 1-chloroethyl carbonochloridate (5 g, 35 mmol) in DCM (100 mL), cyclohexanol (3.9 g, 38.5 mmol) and pyridine (3.3 g, 42 mmol). The title compound was obtained as colorless oil (7 g, 96.9%) and was used in the next step without further purification. The title compound was characterized by 1H NMR as shown below:

Provenance & Evidence