HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90009967, compound → N-(4-(5-Cyclopropyl-3-(4-methyl-5-oxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)pyridin-2-yl)phenyl)-2,6-difluorobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90009967 | HCID 90009967 | — |
| Reactant | HCID 90010642 | HCID 90010642 | — |
| Product | N-(4-(5-Cyclopropyl-3-(4-methyl-5-oxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)pyridin-2-yl)phenyl)-2,6-difluorobenzamide | HCID 72190844 | — |
Reaction Steps
Step-4: N-(4-(5-Bromo-3-(4-methyl-5-oxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)pyridin-2-yl)phenyl)-2,6-difluorobenzamide: The title compound was prepared from ethyl-5-bromo-2-(4-(2,6-difluorobenzamido)phenyl)nicotinate by following the similar procedure sequentially as described in step-2, step-3, and step-4 of Intermediate-1a. ESI-MS (m/z) 487, 489 [(MH)+, Br79,81].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09399638B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-d745bc29b09a4a9396ad65d65f9fdd2f |
| Source note | uspto-grants-2016_07 |