HRID1057501

反应详情

EQUATION

反应方程式

HRID 1057501 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Dimethoxypyridino[3,2-e]pyridin-2-ylmethane was dissolved in methanol (0.5M) followed by addition of 10% Pd/C), and subjected to hydrogenation at ballon pressure. The mixture was filtered through celite and concentrated by rotary evaporation. EI-MS m/z 209 (M+H)+.

WORKUP

后处理

  1. filtrationThe mixture was filtered through celite and
  2. concentrationconcentrated by rotary evaporation