反应详情

To a stirring solution of (2-bromo-5-nitrophenyl) methan-1-ol (1 eq) in methylene chloride (0.1 M) at room temperature was added pyridinium chlorochromate (2 eq). After 2 hr the reaction mixture was filtered through celite and the product was purified by flash chromatography (15% EtOAc/Hexane). EI-MS m/z 230 (M+H)+.

1. filtrationAfter 2 hr the reaction mixture was filtered through celite
2. customthe product was purified by flash chromatography (15% EtOAc/Hexane)