1,2-Dichlorobenzene → 4-(4-Fluorophenoxy)-2-(prop-2-en-1-yl)phenol

Participants

Reaction Steps

4-(4-fluorophenoxy)phenyl allyl ether (4.00 g, 16.37 mmol) was taken up in 1,2-dichlorobenzene (50 mL) and refluxed for 48 h. After cooling, the solvent was removed in vacuo and the resulting crude oil was chromatographed on silica gel (15% ethyl acetate/hexane) to afford the title compound.

Provenance & Evidence