HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Fluorophenoxy)-2-(prop-2-en-1-yl)phenol → 4-(4-Fluorophenoxy)-2-propylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Fluorophenoxy)-2-(prop-2-en-1-yl)phenol | HCID 18672473 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(4-Fluorophenoxy)-2-propylphenol | HCID 18772256 | — |
Reaction Steps
A solution of 4-(4-fluorophenoxy)-2-allylphenol (2.30 g, 9.42 mmol) and 5% Pd/C (0.90 g) in ethyl acetate (30 mL) was stirred under H2 atmosphere for 3 h at room temperature. The reaction mixture was filtered through a short pad of silica gel and concentrated in vacuo to afford the title compound which was used as is.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06515015B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-70b5fe82cc19412f8a4f5ec0e7788ea6 |
| Source note | uspto-grants-2003_02 |