Acetic Acid → HCID 18673077, compound

HRID 1058078Notes

Reaction equation

HRID 1058078 reaction equation
[CH:1]1[CH:6]=[C:5]([CH:7]=O)[C:4]([CH:9]=O)=[CH:3][CH:2]=1.[CH:11]([C:14]1[CH:20]=[CH:19][CH:18]=[C:17]([CH:21]([CH3:23])[CH3:22])[C:15]=1[NH2:16])([CH3:13])[CH3:12].C(O)(=O)C>ClCCl>[CH:21]([C:17]1[CH:18]=[CH:19][CH:20]=[C:14]([CH:11]([CH3:13])[CH3:12])[C:15]=1[N:16]1[CH2:7][C:5]2[C:4](=[CH:3][CH:2]=[CH:1][CH:6]=2)[CH2:9]1)([CH3:23])[CH3:22]

Participants

5

Reactant 3

HCID 176Acetic AcidHCID 4807PhthalaldehydeHCID 32484Diisopropylaniline

Product 1

HCID 18673077HCID 18673077, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

0.5 g of o-phthalaldehyde and 0.661 g of 2,6-diisopropylaniline were dissolved in 20 ml of dichloromethane, 1 ml of acetic acid was added thereto, and the mixture was reacted at room temperature for 25 minutes.

Workup

  1. customthe mixture was reacted at room temperature for 25 minutes

Sources & evidence

ORD record
ord-6e97313963614a84b750cd753f04a775
Source dataset
uspto-grants-2003_02
Patent number
US06515129B1

Reaction notes

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