2,6-Diethylaniline → HCID 9948038, compound

HRID 1058087Notes

Reaction equation

HRID 1058087 reaction equation
[C:1]1(=[O:12])[O:7][C:5](=O)[C:4]2=[CH:8][CH:9]=[CH:10][CH:11]=[C:3]2[CH2:2]1.[CH2:13]([C:15]1[CH:21]=[CH:20][CH:19]=[C:18]([CH2:22][CH3:23])[C:16]=1[NH2:17])[CH3:14]>C(Cl)(Cl)Cl>[CH2:13]([C:15]1[CH:21]=[CH:20][CH:19]=[C:18]([CH2:22][CH3:23])[C:16]=1[N:17]1[C:5](=[O:7])[C:4]2=[CH:8][CH:9]=[CH:10][CH:11]=[C:3]2[CH2:2][C:1]1=[O:12])[CH3:14]

Participants

4

Reactant 2

HCID 113692,6-DiethylanilineHCID 12801Homophthalic anhydride

Product 1

HCID 9948038HCID 9948038, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Conditions

Temperature
180 °C

Procedure

162 mg (1.0 mmol) of homophthalic anhydride and 149 mg (1.0 mmol) of 2,6-diethylaniline were charged in an egg-plant type flask of 50 ml, followed by stirring under heating at a temperature of 180° C. for 2 hours. After cooled, the reactant was dissolved in chloroform, purified by silica gel column chromatography (eluent;

Workup

  1. temperatureAfter cooled
  2. custompurified by silica gel column chromatography (eluent

Sources & evidence

ORD record
ord-db649d528f36428596af62c0037d5230
Source dataset
uspto-grants-2003_02
Patent number
US06515129B1

Reaction notes

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