Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,6-Diethylaniline | HCID 11369 | — |
| Reactant | Homophthalic anhydride | HCID 12801 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 9948038 | HCID 9948038 | — |
Reaction Steps
162 mg (1.0 mmol) of homophthalic anhydride and 149 mg (1.0 mmol) of 2,6-diethylaniline were charged in an egg-plant type flask of 50 ml, followed by stirring under heating at a temperature of 180° C. for 2 hours. After cooled, the reactant was dissolved in chloroform, purified by silica gel column chromatography (eluent;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06515129B1 |
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| Source dataset | uspto-grants-2003_02 |
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| ORD ID | ord-db649d528f36428596af62c0037d5230 |
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| Source note | uspto-grants-2003_02 |
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