HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 88018871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 18668881 | HCID 18668881 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 88018871 | HCID 88018871 | 91% |
Reaction Steps
To a solution of benzyl methoxy-carbonylbenzofuran-2-carboxylate (0.144 g, 0.409 mmol) in ethyl acetate (20 mL) was added 10% palladium on carbon (0.072 g, 50% w/w). After stirring under a hydrogen atmosphere for 2 h, the mixture was filtered through Celite. The filtrate was concentrated to yield the title compound as a white solid (0.098 g, 91%): 1H NMR:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518267B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-88634d6f622e4aaf9fb702900d54b55f |
| Source note | uspto-grants-2003_02 |