HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18668743, compound → 2-(AMINOETHYL)-1-N-BOC-PIPERIDINE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18668743 | HCID 18668743 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(AMINOETHYL)-1-N-BOC-PIPERIDINE | HCID 2756421 | 96.4% |
Reaction Steps
A suspension of 43.0 g of tert-butyl 2-(2-azidoethyl)-1-piperidinecarboxylate and 2.15 g of 5% palladium on carbon in 215 ml of methanol was catalytically hydrogenated at room temperature for 9 hours. After the reaction, the catalyst was filtered off, and the filtrate was concentrated to give 37.2 g of a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518265B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-59645c1470d349f0be47b9938faadc12 |
| Source note | uspto-grants-2003_02 |