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HRID1058767

反应详情

EQUATION

反应方程式

HRID 1058767 的结构方程式

REACTANTS

反应物

2
结构：C=C(Cc1ccc(Br)cc1)C(=O)OCC
HCID12026123

Ethyl 2-(4-bromobenzyl)acrylate

C12H13BrO2

结构：O=C(NC(Cc1ccccc1)[PH](=O)O)OCc1ccccc1
HCID178523200

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C(Cc1ccc(Br)cc1)CP(=O)(O)C(Cc1ccccc1)NC(=O)OCc1ccccc1
HCID18668696

Ethyl 3-(4-bromophenyl)-2-[[hydroxy[2-phenyl-1-[[(phenyl-methoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate

C28H31BrNO6P

收率 84.1%

PROCEDURE

实验过程

The process is performed according to the operating conditions described in 1.6., starting with 2 g (6.27 mmol) of [2-phenyl-1-[(phenylmethoxy)carbonyl]aminoethyl]phosphinic acid synthesized in 1.4. and 2 g (7.44 mol) of ethyl 4-bromo-α-methylenebenzenepropanoate. 3.1 g of product are recovered (yield=84.1%)

WORKUP

后处理

  1. customsynthesized in 1.4
  2. custom3.1 g of product are recovered (yield=84.1%)