HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 23562520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 69939850 | HCID 69939850 | — |
| Product | HCID 23562520 | HCID 23562520 | 98% |
Reaction Steps
Phenylmethyl N- [2 -[[hydroxy [2 -phenyl-1-[[(tert-butoxy) carbonyl]amino]ethyl]phosphinyl]methyl]-1-oxo-3-phenylpropyl]-L-phenylalaninate is treated with a trifluoroacetic acid/dichloromethane mixture for one hour at room temperature. The mixture is evaporated to dryness. The product obtained is precipitated from ether. The product is recovered in a yield of 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518260B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-57b8ca1e6198435da6db2a7cee8d8b92 |
| Source note | uspto-grants-2003_02 |