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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1058774Generated: November 1, 2026

Trifluoroacetic acid methylene chloride → HCID 23562520, compound

https://huagongshe.com/reaction/1058774

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acid methylene chlorideHCID 21863450—
ReactantHCID 69939850HCID 69939850—
ProductHCID 23562520HCID 2356252098%

Reaction Steps

Phenylmethyl N- [2 -[[hydroxy [2 -phenyl-1-[[(tert-butoxy) carbonyl]amino]ethyl]phosphinyl]methyl]-1-oxo-3-phenylpropyl]-L-phenylalaninate is treated with a trifluoroacetic acid/dichloromethane mixture for one hour at room temperature. The mixture is evaporated to dryness. The product obtained is precipitated from ether. The product is recovered in a yield of 98%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06518260B1
Source datasetuspto-grants-2003_02
ORD IDord-57b8ca1e6198435da6db2a7cee8d8b92
Source noteuspto-grants-2003_02