HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69940123, compound → HCID 23562522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69940123 | HCID 69940123 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 23562522 | HCID 23562522 | 97% |
Reaction Steps
Phenylmethyl N-[2-[[[2-phenyl-1-[[(tert-butoxy)carbonyl]amino]ethyl]phenylmethoxyphosphinyl]methyl]-1-oxo-3-phenylpropyl]-L-phenylalaninate is stirred for 2 hours in the presence of formic acid. The mixture is evaporated to dryness. The product is precipitated using diethyl ether. The product is recovered in a yield of 97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518260B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-93fd57dfb87847df83ab7482f5382d76 |
| Source note | uspto-grants-2003_02 |